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HRID 324149作成日:2026年10月25日

Benzyl 4-n-dodecylcarbonyloxybenzoate → 4-n-Dodecylcarbonyloxybenzoic acid

https://huagongshe.com/reaction/324149

反応式

関与物質

役割名称HCID仕込み量
反応物Benzyl 4-n-dodecylcarbonyloxybenzoateHCID 22002898—
触媒PalladiumHCID 23938—
溶媒Ethyl AcetateHCID 8857—
生成物4-n-Dodecylcarbonyloxybenzoic acidHCID 2200287387%

反応手順

{circle around (2)}: A mixture comprising 3.5 g of benzyl 4-n-dodecylcarbonyloxybenzoate, 0.4 g of palladium/carbon and 20 g of ethyl acetate was stirred for 6 hours under hydrogen atmosphere. Then, palladium/carbon was filtered off, and ethyl acetate was distilled off from the filtrate. The resultant residue was recrystallized from toluene, whereby 2.40 g of 4-n-dodecylcarbonyloxybenzoic acid was obtained in the form of a colorless crystal.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06217793B1
出典データセットuspto-grants-2001_04
ORD IDord-6d4cec3c86ba4e7e8177b7e1ef0d4e52
出典メモuspto-grants-2001_04