HCID 86756615, compound → HCID 54393751, compound

Participants

Reaction Steps

{circle around (2)}: A mixture comprising 2.2 g of (S)-4-[4′-(1″-methylheptyloxy)phenylcarbonyloxy)-1-benzyloxybenzene, 0.2 g of palladium/carbon and 10 g of ethyl acetate was stirred for 6 hours under hydrogen atmosphere. Then, palladium/carbon was filtered off, followed by distilling off ethyl acetate from the filtrate. The resultant residue was recrystallized from hexane, whereby 1.1 g of (S)-4-[4′-(1″-methylheptyloxy)phenylcarbonyloxy)phenol was obtained in the form of a colorless crystal.

Provenance & Evidence