HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentanone → HCID 69310695, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentanone | HCID 8452 | — |
| Reactant | HCID 69307898 | HCID 69307898 | — |
| Product | HCID 69310695 | HCID 69310695 | — |
Reaction Steps
Using alkylation method A, 3-chloro-N-[(R)-1-phenyl-2-(piperidin-4-ylmethoxy)ethyl]-1H-indole-6-carboxamide hydrochloride (150 mg, 0.33 mmol) and cyclopentanone (0.5 mL, 5.7 mmol) afforded, after purification (SiO2: 8:2:1 hexane:EtOAc:isopropylamine), 78 mg (49%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07427632B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-ddafbea0ff66414887357da8f5cd99ea |
| Source note | uspto-grants-2008_09 |