HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromothiophene → HCID 10800660, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromothiophene | HCID 13383 | — |
| Reactant | 2-Bromothiophene | HCID 13851 | — |
| Reactant | 4-Methoxy-2-nitroaniline | HCID 66793 | — |
| Product | HCID 10800660 | HCID 10800660 | — |
Reaction Steps
Reaction of 4-methoxy-2-nitroaniline (X:R=4-OMe) and 3-bromothiophene (XI:R′=3-Br) as described above for Example 55, but for only 6 hours, gave 4-methoxy-2-nitro-N-(3-thienyl)aniline (XIV:R′=4-OMe, 3-thienyl) (71%): mp (EtOAc/petroleum ether) 121-123° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06218388B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-c9def635c0c541f9929c4b2ed4f5936b |
| Source note | uspto-grants-2001_04 |