Methanol → HCID 86757899, compound

Participants

Reaction Steps

3-(3,4-Difluorophenyl)-2-methyl-5-oxo-morpholine-4-carboxylic acid-4-nitro-phenyl ester (section II, part 1) was coupled to 3-[4-(cyano-4-phenyl-piperidin-1-yl]-propylamine in the same manner as described in section I, part 3c. White powder. M.P.=191-194° C.; Mass spec. 497 (M+1, 100%); [α]D=+23.1 (c=0.09, MeOH) Analysis calculated for C33H36N3O4F2Cl.0.35 CH2Cl2: C, 58.38; H, 5.68; N, 9.96. Found: C, 58.57; H, 6.03; N, 9.72.

Provenance & Evidence