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HRID324396

反应详情

EQUATION

反应方程式

HRID 324396 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)c1coc(CBr)n1
HCID641223

ethyl 2-(bromomethyl)-1,3-oxazole-4-carboxylate

C7H8BrNO3

结构：CCc1nc2c(o1)C=Cc1cc(C)ccc1C2c1c[nH]c(=O)[nH]c1=O
HCID70112980

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1coc(Cn2cc(C3c4ccc(C)cc4C=Cc4oc(CC)nc43)c(=O)[nH]c2=O)n1
HCID131722501

未命名化合物

PROCEDURE

实验过程

The subtitle compound was prepared from the product from example 1 step (vii) (6.5 g) and 2-[bromomethyl]-4-oxazolecarboxylic acid ethyl ester (Coll. Czech Chem. Comm., 1967, 32, 2155) (1.69 g) by the method of example 1 step (viii). Purification was by chromatography eluting with 60-66% ethyl acetate in toluene.

WORKUP

后处理

  1. customPurification
  2. washeluting with 60-66% ethyl acetate in toluene