HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 69313249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 3-Chloro-N-[1-(2-pyridinyl)-2-(1-isopropylpiperidin-4-yl-methoxy)ethyl]-1H-indole-6-carboxamide | HCID 69307937 | — |
| Product | HCID 69313249 | HCID 69313249 | 179.1% |
Reaction Steps
Using deprotection method A, 3-chloro-N-[1-(2-pyridinyl)-2-(1-isopropylpiperidin-4-ylmethoxy)ethyl]-1H-indole-6-carboxamide (105 mg, 0.25 mmol) and acetone (1.2 mL, 16.8 mmol) afforded 110 mg (96%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07427632B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-93a9cac0e14348288f94a2a269732aa8 |
| Source note | uspto-grants-2008_09 |