HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-1H-indole-6-carboxylic acid → HCID 44444042, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-1H-indole-6-carboxylic acid | HCID 15543042 | — |
| Reactant | HCID 69307860 | HCID 69307860 | — |
| Product | HCID 44444042 | HCID 44444042 | — |
Reaction Steps
Using coupling method A, crude 4-(1-isopropylpiperidin-4-yl)-1-phenylbutylamine hydrochloride (0.70 mmol) and 3-chloroindole-6-carboxylic acid (162 mg, 0.83 mmol) afforded, after purification (SiO2: 10:10:1 hexane:EtOAc:isopropylamine), 66 mg (13%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07427632B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-927e06a3a3694ca0a9f621a8821f9743 |
| Source note | uspto-grants-2008_09 |