HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 29938143, compound → Ethyl 3-(2,3-dihydrobenzofuran-5-yl)propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 29938143 | HCID 29938143 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 3-(2,3-dihydrobenzofuran-5-yl)propanoate | HCID 11053175 | 99.4% |
Reaction Steps
5% Palladium-carbon (1 g, containing 50% water) was added to an ethanol (150 ml) solution of ethyl (E)-3-(2.3-dihydrobenzofuran-5-yl)-2-propenoate (14.7 g, 66.7 mmols), and the mixture was stirred in a hydrogen atmosphere at room temperature for 2 hours. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to obtain 14.6 g (yield: 99%) of the target compound. This was oily.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06218429B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-816c5ca6c4e441a29d6d845e8883a12d |
| Source note | uspto-grants-2001_04 |