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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 324607Generated: October 28, 2026

HCID 29938143, compound → Ethyl 3-(2,3-dihydrobenzofuran-5-yl)propanoate

https://huagongshe.com/reaction/324607

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 29938143HCID 29938143—
ReactantHCID 178418361HCID 178418361—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductEthyl 3-(2,3-dihydrobenzofuran-5-yl)propanoateHCID 1105317599.4%

Reaction Steps

5% Palladium-carbon (1 g, containing 50% water) was added to an ethanol (150 ml) solution of ethyl (E)-3-(2.3-dihydrobenzofuran-5-yl)-2-propenoate (14.7 g, 66.7 mmols), and the mixture was stirred in a hydrogen atmosphere at room temperature for 2 hours. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to obtain 14.6 g (yield: 99%) of the target compound. This was oily.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06218429B1
Source datasetuspto-grants-2001_04
ORD IDord-816c5ca6c4e441a29d6d845e8883a12d
Source noteuspto-grants-2001_04