HCID 67483670, compound → HCID 53716329, compound

Participants

Reaction Steps

The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a mixture of olefin isomers): δ 0.73 (t, J=7.0 Hz, 3 H), 1.10-1.40 (m, 18 H), 1.91 (tdd, J=7.0, 7.0, 1.0, 2 H), 2.68 (q, J=7.4 Hz, 2 H), 3.3-3.5 (m, 2 H), 4.41 (d, J=5.5 Hz, 2 H), 5.20-5.40 (m, 1 H), 6.0 (dt, J=16.0, 1.0 Hz, 1 H), 7.0 (d, J=8.5 Hz, 2 H), 7.23 (d, J=8.5 Hz, 2 H). FAB-MS: calculated for C25H35NO 366; found 366 (M+H, 100%). Rf=0.31 (10% ethyl acetate/n-hexane).

Provenance & Evidence