HCID 53716329, compound → HCID 22005154, compound

Participants

Reaction Steps

The title compound was prepared from 2,6-diisopropyl-3-hydroxymethyl-4-(4ethylphenyl)5(pent-1-enyl)pyridine (Example 131) by the procedure described in Example 126. 1H NMR (300 MHz, CDCl3): δ 0.77 (t, J=7.0 Hz, 3 H), 1.0-1.40 (m, 22 H), 2.28 (m, 2 H), 2.73 (q, J=7.5 Hz, 2 H), 3.35 (m, 1 H), 3.45 (m, 1 H), 4.35 (s, 2 H), 7.10 (d, J=8.0 Hz, 2 H), 7.18-7.34 (d, J=8.0 Hz, 2 H). FAB-MS: calculated for C25H37NO 368; found 368 (M+H, 100%). Rf=0.31 (10% ethyl acetate/n-hexane). mp 87-88° C.

Provenance & Evidence