Ammonium Hydroxide → HCID 54118004, compound

Participants

Reaction Steps

Prepared from 4-phenylbenzaldehyde, ethyl isobutyrylacetate and concentrated ammonium hydroxide by the procedures described in Example 125, Steps A-E. 1H NMR (300 MHz, CDCl3): δ 0.73 (t, J=7.4 Hz, 3 H), 0.93 (t, J=7.0 Hz, 3 H), 1.10-1.40 (m, 14 H), 1.97 (tdd, J=7.0, 7.0, 1.1 Hz, 2 H), 3.10 (m, 1 H), 3.45 (m, 1 H), 4.0 (q, J=7.4 Hz, 2 H), 5.40 (m, 1 H), 6.10 (dt, J=16.2, 1.1 Hz, 1 H), 7.20-7.70 (m, 9 H). mp 104-106° C.

Provenance & Evidence