HCID 67483736, compound → HCID 53889227, compound

Participants

Reaction Steps

The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a mixture of olefins): δ 0.73 (t, J=7.0 Hz, 3 H), 1.10-1.40 (m, 15 H), 1.90 (tdd, J=7.0, 7.0, 1.0, 2 H), 2.36 (s, 3 H), 3.30-3.50 (m, 21 H), 4.40 (d, J=4.0 Hz, 2 H), 5.20-5.40 (m, 1 H), 5.95 (dt, J=16.0, 1.0 Hz, 1 H), 6.90 (m, 2 H), 7.10-7.30 (m, 2 H). FAB-MS: calculated for C24H33NO 352; found 352 (M+H, 100%). Rf=0.34 (10% ethyl acetate/n-hexane). mp 94-97° C.

Provenance & Evidence