HCID 53889227, compound → HCID 22005070, compound

Participants

Reaction Steps

The title compound was prepared from 2,6-diisopropyl-3-hydroxymethyl-4-(3-methylphenyl)-5-(pent-1-enyl)pyridine (Example 139) by the procedure described in Example 126. 1H NMR (300 MHz, CDCl3): δ 0.77 (t, J=7.0 Hz, 3 H), 1.0-1.40 (m, 19 H), 2.25 (m, 2 H), 2.39 (s, 3 H), 3.23 (m, 1 H), 3.44 (m, 1 H), 4.34 (s, 2 H), 6.97 (m, 2 H), 7.18-7.34 (m, 2 H). FAB-MS: calculated for C24H35NO 354; found 354 (M+H, 100 %). Rf=0.34 (10% ethyl acetate/n-hexane). mp 88-90° C.

Provenance & Evidence