HCID 53963478, compound → HCID 22005361, compound

Participants

Reaction Steps

The title compound was prepared from 2,6-diisopropyl-3-hydroxymethyl-4-(4-chlorophenyl)-5(pent-1-enyl)pyridine (Example 143) by the procedure described in Example 126. 1H NMR (300 MHz, CDCl3): δ 0.79 (t, J=7.0 Hz, 3 H), 1.08-1.38 (m, 18 H), 2.26 (m, 2 H), 3.22 (m, 1 H), 3.40 (m, 1 H), 4.31 (d, J=5.0 Hz, 1 H), 7.13 (d, J=8.0 Hz, 2 H), 7.42 (d, J=8.0 Hz, 2 H). mp 83-85° C. Rf=0.36 (10% ethyl acetate/n-hexane).

Provenance & Evidence