HCID 67483305, compound → HCID 54469891, compound

Participants

Reaction Steps

The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a mixture of olefin isomers): δ 0.75 (t, J=7.5 Hz, 3 H), 1.10-1.40 (m, 15 H), 1.93 (tdd, J=7.0, 7.0, 1.0 Hz, 2 H) 3.30-3.50 (m, 2 ), 4.37 (d, J=12.0 Hz, 1 H), 4.43 (d, J=12.0 Hz, 1 H), 5.20-5.40 (m, 1 H), 5.9 (dt, J=16.0, 1.1 Hz, 1 H), 7.0-7.40 (m, 4 H). FAB-MS: calculated for C23H30NOCl 372; found 372 (M+H, 100%). Rf=0.26 (10% ethyl acetate/n-hexane). mp 101-104° C.

Provenance & Evidence