HCID 54517473, compound → HCID 22005146, compound

Participants

Reaction Steps

The title compound was prepared from 2,6-diisopropyl-3-hydroxymethyl-4-(2,4-dichlorophenyl)-5-(pent-1-enyl)pyridine (Example 147) by the procedure described in Example 126. 1H NMR (300 MHz, CDCl3): δ 0.80 (t, J=7.0 Hz, 3 H), 1.12-1.48 (m, 18 H), 2.12 (m, 1 H), 2.35 (m, 1 H), 3.26 (m, 1 H) 3.45 (m, 1 H), 4.31 (AB, J=12.0 Hz, 2 H), 7.16 (d, J=8.0 Hz, 1 H), 7.36 (dd, J=8.0, 2.0 Hz, 1 H), 7.54 (d, J=2.0, 1 H). Rf0.38 (10% ethyl acetate/n-hexane).

Provenance & Evidence