HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 21709154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 4-Methyl-2-phenylpyridine | HCID 77026 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 21709154 | HCID 21709154 | — |
Reaction Steps
To a solution of 100 mg of 2-phenyl-4-methylpyridine in 2 mL of carbon tetrachloride was added 300 mg of sodium carbonate and 100 mg of bromine. The reaction mixture was stirred and irradiated with a 500 W lamp for 1 h, filtered and the solvent removed by evaporation under reduced pressure to yield 2-phenyl-4-bromomethylpyridine which was used in the next step without further purification or characterization
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06221871B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-91aae9b73cce4d53b6adba559b6a7db8 |
| Source note | uspto-grants-2001_04 |