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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 324972Generated: October 29, 2026

Sodium Carbonate → HCID 21709154, compound

https://huagongshe.com/reaction/324972

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium CarbonateHCID 10340—
ReactantBromineHCID 24408—
Reactant4-Methyl-2-phenylpyridineHCID 77026—
SolventCarbon TetrachlorideHCID 5943—
ProductHCID 21709154HCID 21709154—

Reaction Steps

To a solution of 100 mg of 2-phenyl-4-methylpyridine in 2 mL of carbon tetrachloride was added 300 mg of sodium carbonate and 100 mg of bromine. The reaction mixture was stirred and irradiated with a 500 W lamp for 1 h, filtered and the solvent removed by evaporation under reduced pressure to yield 2-phenyl-4-bromomethylpyridine which was used in the next step without further purification or characterization

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06221871B1
Source datasetuspto-grants-2001_04
ORD IDord-91aae9b73cce4d53b6adba559b6a7db8
Source noteuspto-grants-2001_04