HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 21709149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21709156 | HCID 21709156 | — |
| Product | HCID 21709149 | HCID 21709149 | — |
Reaction Steps
A solution of 55 mg 2-phenyl-4-hydroxymethylpyrimidine in 1 mL of thionyl chloride was heated at reflux temperature for 1 hr and the excess thionyl chloride removed by evaporation under reduced pressure to yield 50 mg of 2-phenyl-4-chloromethylpyrimidine as an oil which was used in the next step without further purification or characterization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06221871B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-3caf94b9aac94bb6b5bcf38ecb8911eb |
| Source note | uspto-grants-2001_04 |