HRID325007

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2777240

5-Chlorosulfonyl-2-hydroxybenzoic acid

C7H5ClO5S

结构：Oc1ccc(-c2ccc(-c3c(Cc4ccccc4)oc4ccccc34)cc2)cc1

HCID10547545

未命名化合物

PRODUCTS

生成物

结构：O=C(O)c1cc(S(=O)(=O)Oc2ccc(-c3ccc(-c4c(Cc5ccccc5)oc5ccccc45)cc3)cc2)ccc1O

HCID9808280

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from of 4′-(2-benzyl-benzofuran-3-yl)-biphenyl-4-ol and 5-chlorosulfonyl-2-hydroxy-benzoic acid, in substantially the same manner, as described in Example 1 step g, and was obtained as a white solid, mp 171-173° C.; MS m/e 575 (M-H)+;

WORKUP

后处理

customwas obtained as a white solid, mp 171-173° C.

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-c991ad2ec14b4cfab41830a105296835
来源数据集: uspto-grants-2001_04
DOI: 10.6084/m9.figshare.5104873.v1
专利: US06221902B1
来源说明: uspto-grants-2001_04

反应 SMILES

[CH2:1]([C:8]1[O:9][C:10]2[CH:29]=[CH:28][CH:27]=[CH:26][C:11]=2[C:12]=1[C:13]1[CH:18]=[CH:17][C:16]([C:19]2[CH:24]=[CH:23][C:22]([OH:25])=[CH:21][CH:20]=2)=[CH:15][CH:14]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[S:31]([C:34]1[CH:35]=[CH:36][C:37]([OH:43])=[C:38]([CH:42]=1)[C:39]([OH:41])=[O:40])(=[O:33])=[O:32]>>[CH2:1]([C:8]1[O:9][C:10]2[CH:29]=[CH:28][CH:27]=[CH:26][C:11]=2[C:12]=1[C:13]1[CH:18]=[CH:17][C:16]([C:19]2[CH:24]=[CH:23][C:22]([O:25][S:31]([C:34]3[CH:35]=[CH:36][C:37]([OH:43])=[C:38]([CH:42]=3)[C:39]([OH:41])=[O:40])(=[O:33])=[O:32])=[CH:21][CH:20]=2)=[CH:15][CH:14]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1