HCID 10788310, compound → HCID 9895320, compound

HRID 325011Notes

Reaction equation

HRID 325011 reaction equation
[CH2:1]([C:8]1[O:9][C:10]2[CH:32]=[CH:31][CH:30]=[CH:29][C:11]=2[C:12]=1[C:13]1[CH:18]=[CH:17][C:16]([C:19]2[CH:24]=[CH:23][C:22]([OH:25])=[C:21]([N+:26]([O-:28])=[O:27])[CH:20]=2)=[CH:15][CH:14]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[S:34]([C:37]1[CH:45]=[CH:44][C:40]([C:41]([OH:43])=[O:42])=[C:39]([OH:46])[CH:38]=1)(=[O:36])=[O:35]>>[CH2:1]([C:8]1[O:9][C:10]2[CH:32]=[CH:31][CH:30]=[CH:29][C:11]=2[C:12]=1[C:13]1[CH:14]=[CH:15][C:16]([C:19]2[CH:24]=[CH:23][C:22]([O:25][S:34]([C:37]3[CH:45]=[CH:44][C:40]([C:41]([OH:43])=[O:42])=[C:39]([OH:46])[CH:38]=3)(=[O:36])=[O:35])=[C:21]([N+:26]([O-:28])=[O:27])[CH:20]=2)=[CH:17][CH:18]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 10788310HCID 10788310, compoundHCID 146685314-(Chlorosulfonyl)-2-hydroxybenzoic acid

Product 1

HCID 9895320HCID 9895320, compound

Procedure

The title compound was prepared from 4′-(2-benzyl-benzofuran-3-yl)-3-nitro-biphenyl-4-ol and 4-chlorosulfonyl-2-hydroxy-benzoic acid, in substantially the same manner, as described in Example 1 step g, and was obtained as a yellow solid, mp 200° C.; MS m/e 620 (M-H)+;

Workup

  1. customwas obtained as a yellow solid, mp 200° C.

Sources & evidence

ORD record
ord-f4f76a97e9174e88a8967ca575a5047a
Source dataset
uspto-grants-2001_04
Patent number
US06221902B1

Reaction notes

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