HCID 10790583, compound → HCID 9917827, compound

HRID 325015Notes

Reaction equation

HRID 325015 reaction equation
[CH2:1]([C:8]1[S:12][C:11]2[CH:13]=[CH:14][CH:15]=[CH:16][C:10]=2[C:9]=1[C:17]1[CH:22]=[CH:21][C:20]([C:23]2[CH:28]=[CH:27][C:26]([OH:29])=[C:25]([Br:30])[CH:24]=2)=[CH:19][CH:18]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[S:32]([C:35]1[CH:43]=[CH:42][C:38]([C:39]([OH:41])=[O:40])=[C:37]([OH:44])[CH:36]=1)(=[O:34])=[O:33]>>[CH2:1]([C:8]1[S:12][C:11]2[CH:13]=[CH:14][CH:15]=[CH:16][C:10]=2[C:9]=1[C:17]1[CH:22]=[CH:21][C:20]([C:23]2[CH:28]=[CH:27][C:26]([O:29][S:32]([C:35]3[CH:43]=[CH:42][C:38]([C:39]([OH:41])=[O:40])=[C:37]([OH:44])[CH:36]=3)(=[O:34])=[O:33])=[C:25]([Br:30])[CH:24]=2)=[CH:19][CH:18]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 10790583HCID 10790583, compoundHCID 146685314-(Chlorosulfonyl)-2-hydroxybenzoic acid

Product 1

HCID 9917827HCID 9917827, compound

Procedure

The title compound was prepared from 4′-(2-benzyl-benzo[b]thiophen-3-yl)-3-bromo-biphenyl-4-ol and 4-chlorosulfonyl-2-hydroxy-benzoic acid, in substantially the same manner, as described in Example 1 step g, and was obtained as an off-white solid, mp 117-119° C.; MS m/e 669 (M-H)+;

Workup

  1. customwas obtained as an off-white solid, mp 117-119° C.

Sources & evidence

ORD record
ord-87df7d77755a4667a6bf7399b11ff6ed
Source dataset
uspto-grants-2001_04
Patent number
US06221902B1

Reaction notes

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