HCID 69592311, compound → HCID 69592294, compound

Participants

Reaction Steps

A suspension of 3-[2-(4-amino{t-butoxycarbonylimino}methylphenyl)-ethoxy]nitrobenzene (1.47 g; 3.81 mmol; from step (iii) above) and Pd (0.236 g; 5% on charcoal) in EtOH (75 mL) was stirred under H2(g) (1 atm.) for 25 minutes. After filtration through Celite the solvent was evaporated. The residue was purified by preparative HPLC (60% CH3CN/aq:0.1M NH4OAc) to afford the sub-title compound. Yield: 1.02 g (75%).

Provenance & Evidence