HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 3089143, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 2-Amino-4-Nitrophenol | HCID 3613389 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 3089143 | HCID 3089143 | — |
Reaction Steps
About 60 grams (0.3 mole) of the 4-nitrophenylchloroxime is mixed with 340 milliliters of ethanol, 60 grams (0.39 moles) of 2-amino-4-nitrophenol and 60 milliliters of dimethylformamide. The mixture is heated to reflux for about 6.5 hours, filtered, washed with methanol and air dried. Approximately 55 grams of 2-(p-nitrophenyl)-5-nitrobenzoxazole are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06222044B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-85d0df421a9843b1ad9f143fa8732c36 |
| Source note | uspto-grants-2001_04 |