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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 325087Generated: October 29, 2026

Ethanol → HCID 4137682, compound

https://huagongshe.com/reaction/325087

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
Reactant2-Amino-4-NitrophenolHCID 3613389—
ProductHCID 4137682HCID 4137682—

Reaction Conditions

Temperature30 °C

Reaction Steps

To 11.5 grams (0.05 mole) of 3-nitrophenylchloroxime are added 150 milliliters of ethanol. To the mixture are added 23.1 grams (0.15 moles) of 2-amino-4-nitrophenol. The mixture is stirred under nitrogen at about 30° C. overnight and filtered to yield 2-(m-nitrophenyl)-5-nitrobenzoxazole.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06222044B1
Source datasetuspto-grants-2001_04
ORD IDord-6bcc65375dca4547aa9a0e22bc3c1921
Source noteuspto-grants-2001_04