HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyaniline → N-(2-Methoxyphenyl)benzeneethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyaniline | HCID 7000 | — |
| Reactant | Styrene | HCID 7501 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | N-(2-Methoxyphenyl)benzeneethanamine | HCID 9815989 | 85% |
Reaction Steps
According to GWM, 0.011 mol (=1.25 ml) of o-anisidine and 0.011 mol (=1.25 ml) of styrene are reacted with one another. The product is isolated by column chromatography using ethyl acetate/n-hexane (1:5) as eluent, the product N-(2-phenylethyl)-(o-methoxy)aniline being obtained as a slightly pink liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06222073B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-f7aa953ef03b44a78e978fee00d53d46 |
| Source note | uspto-grants-2001_04 |