HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → N-(1-phenylpropan-2-yl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | beta-Methylstyrene | HCID 12500 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | N-(1-phenylpropan-2-yl)aniline | HCID 418677 | 50% |
Reaction Steps
According to GWM, 0.011 mol (=1.00 ml) of aniline and 0.011 mol (=1.43 ml) of β-methylstyrene are reacted with one another. The product is isolated by column chromatography using ethyl acetate/n-hexane (1:10) as eluent, the product (±)-N-(1-methyl-2-phenylethyl)aniline being obtained as a slightly pink liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06222073B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-420bf818c81e476abec20c16eaf4a5f7 |
| Source note | uspto-grants-2001_04 |