HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3,4-dimethoxybenzyl)-N-[thieno[2,3-d]pyrimidin-6-ylmethylidene]amine → 6-[1-(3,4-Dimethoxybenzyl)-4-phenyl-1H-imidazol-5-yl]-4-(methylthio)thieno[2,3-d]pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3,4-dimethoxybenzyl)-N-[thieno[2,3-d]pyrimidin-6-ylmethylidene]amine | HCID 17965764 | — |
| Reactant | N-(3,4-dimethoxybenzyl)-N-{[4-(methylthio)thieno[2,3-d]pyrimidin-6-yl]methylidene}amine | HCID 69195986 | — |
| Product | 6-[1-(3,4-Dimethoxybenzyl)-4-phenyl-1H-imidazol-5-yl]-4-(methylthio)thieno[2,3-d]pyrimidine | HCID 17965760 | 55% |
Reaction Steps
The title compound was prepared in 55% yield using a procedure similar to the one described for example 6 above but starting from N-(3,4-dimethoxybenzyl)-N-{[4-(methylthio)thieno[2,3-d]pyrimidin-6-yl]methylidene}amine (intermediate 18) (76 mg), in place of N-(3,4-dimethoxybenzyl)-N-[thieno[2,3d]pyrimidin-6-ylmethylidene]amine (intermediate 14);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07427616B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-8db58ff812ce41e083de97f866f31b2c |
| Source note | uspto-grants-2008_09 |