N-(3,4-dimethoxybenzyl)-N-[thieno[2,3-d]pyrimidin-6-ylmethylidene]amine → N-(3,4-dimethoxybenzyl)-N-{[4-(methylthio)thieno[2,3-d]pyrimidin-6-yl]methylidene}amine

HRID 32525Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 32525
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:18]=[CH:19][C:20]=1[O:21][CH3:22])[CH2:6][N:7]=[CH:8][C:9]1[S:17][C:12]2[N:13]=[CH:14][N:15]=[CH:16][C:11]=2[CH:10]=1.[CH3:23][S:24]C1C2C=C(C=O)SC=2N=CN=1.N1C2SC(C=O)=CC=2C=NC=1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:18]=[CH:19][C:20]=1[O:21][CH3:22])[CH2:6][N:7]=[CH:8][C:9]1[S:17][C:12]2[N:13]=[CH:14][N:15]=[C:16]([S:24][CH3:23])[C:11]=2[CH:10]=1

Komponenten

4

Edukt 3

HCID 17965764N-(3,4-dimethoxybenzyl)-N-[thieno[2,3-d]pyrimidin-6-ylmethylidene]amineHCID 17965793Thieno[2,3-d]pyrimidine-6-carbaldehydeHCID 179658594-(Methylthio)thieno[2,3-d]pyrimidine-6-carbaldehyde2×

Produkt 1

HCID 69195986N-(3,4-dimethoxybenzyl)-N-{[4-(methylthio)thieno[2,3-d]pyrimidin-6-yl]methylidene}amine

Versuchsvorschrift

The title compound was prepared by a similar process to that described for Intermediate 14 but using 4-(methylthio)thieno[2,3-d]pyrimidine-6-carbaldehyde (intermediate 15) in place of thieno[2,3-d]pyrimidine-6-carbaldehyde (intermediate 13). White solid (76 mg, 97%);

Quellen und Nachweise

ORD-Eintrag
ord-af57e5d0c78d44328c13532ca3ba0ae9
Quelldatensatz
uspto-grants-2008_09
Patentnummer
US07427616B2

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