Acetic Anhydride → HCID 13017506, compound

HRID 325291Notes

Reaction equation

HRID 325291 reaction equation
[CH3:1][C:2]1[C:11]([C:12](O)=[O:13])=[C:10]([C:15]([OH:17])=[O:16])[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([CH3:18])[CH:8]=2)[N:3]=1.C(OC(=O)C)(=O)C>>[CH3:1][C:2]1[C:11]2[C:12]([O:16][C:15](=[O:17])[C:10]=2[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([CH3:18])[CH:8]=2)[N:3]=1)=[O:13]

Participants

3

Reactant 2

HCID 7918Acetic AnhydrideHCID 13017505HCID 13017505, compound

Product 1

HCID 13017506HCID 13017506, compound

Procedure

A 2 L round bottom flask fitted with a magnetic stirring bar, reflux condenser, and drying tube was charged with 70 g (0.285 mole) of (i) and 1 L of reagent grade acetic anhydride. The tan suspension was stirred at reflux for 23 hours.

Workup

  1. customA 2 L round bottom flask fitted with a magnetic stirring bar
  2. temperaturereflux condenser
  3. customdrying tube
  4. temperatureat reflux for 23 hours

Sources & evidence

ORD record
ord-1e892f2fcfc74db0b04f7d0ad31d4319
Source dataset
uspto-grants-1984_04
Patent number
US04440768

Reaction notes

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