Acetic Anhydride → HCID 15154343, compound

HRID 325292Notes

Reaction equation

HRID 325292 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[N:8]=[C:7]([CH3:12])[C:6]([C:13]([OH:15])=O)=[C:5]2[C:16]([OH:18])=[O:17].CC(OC(C)=O)=O>>[Br:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[N:8]=[C:7]([CH3:12])[C:6]1[C:13]([O:18][C:16](=[O:17])[C:5]2=1)=[O:15]

Participants

3

Reactant 2

HCID 7918Acetic AnhydrideHCID 4394155HCID 4394155, compound

Product 1

HCID 15154343HCID 15154343, compound

Procedure

A 1 liter round-bottom flask with a magnetic stirring bar, reflux condenser and drying tube was charged with 16 g (0.0516 mole) of (viii) and 250 ml of reagent grade Ac2O. The mixture was stirred and refluxed for 18 hours.

Workup

  1. temperatureA 1 liter round-bottom flask with a magnetic stirring bar, reflux condenser
  2. customdrying tube
  3. temperaturerefluxed for 18 hours

Sources & evidence

ORD record
ord-d6dcfae641b14266b14bae2a1a9550fa
Source dataset
uspto-grants-1984_04
Patent number
US04440768

Reaction notes

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