HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Acetylthio-3-methylbenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 3-Methyl-2-sulfanylbenzoic acid | HCID 12612808 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2-Acetylthio-3-methylbenzoic acid | HCID 20465213 | — |
Reaction Steps
2-Mercapto-3-methylbenzoic acid (9.0 g, 54 mmol), acetic anhydride (6.5 g, 63 mmol) and glacial acetic acid (25 ml) were refluxed 1 hour, then poured into dilute hydrochloric acid. The product was filtered and recrystallized from toluene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04440941 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-6715ab2fd23843db950559761faa08af |
| Source note | uspto-grants-1984_04 |