HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-Acetylthio-3-methylbenzoyl)-N-cyclopentylglycine → N-(2-Mercapto-3-methylbenzoyl)-N-cyclopentylglycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-Acetylthio-3-methylbenzoyl)-N-cyclopentylglycine | HCID 13298946 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | N-(2-Mercapto-3-methylbenzoyl)-N-cyclopentylglycine | HCID 20465231 | — |
Reaction Steps
To a chilled solution of methanolic ammonia (30 ml) was added 2.6 g (0.0078 mole) of N-(2-acetylthio-3-methylbenzoyl)-N-cyclopentylglycine. The reaction was covered with a nitrogen atmosphere and stirred three hours while warming slowly from 0° C. to room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04440941 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-e432d0224b8049d28d5e95380af8a551 |
| Source note | uspto-grants-1984_04 |