HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-Acetylthio-3-chlorobenzoyl)-N-cyclopentylglycine → N-(3-Chloro-2-sulfanylbenzoyl)-N-cyclopentylglycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-Acetylthio-3-chlorobenzoyl)-N-cyclopentylglycine | HCID 13051352 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | N-(3-Chloro-2-sulfanylbenzoyl)-N-cyclopentylglycine | HCID 13051353 | — |
Reaction Steps
To a chilled solution of methanolic ammonia (50 ml) was added 3.7 g (0.0104 m) of N-(2-acetylthio-3-chlorobenzoyl)-N-cyclopentylglycine. The reaction was covered with nitrogen and stirred 3 hours while warming slowly from 0° C. to room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04440941 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-da84fe60c942407e8f99e9fa3dbaa523 |
| Source note | uspto-grants-1984_04 |