HCID 23312524, compound → HCID 23312521, compound

HRID 325516Notes

Reaction equation

HRID 325516 reaction equation
NC1C(NCCSCC2C=C(CN(C)C)SC=2)=NS(=O)N=1.[NH2:22][C:23]1[C:27]([NH:28][CH2:29][CH2:30][S:31][CH2:32][C:33]2[S:34][C:35]([CH2:39][N:40]([CH3:42])[CH3:41])=[C:36]([CH3:38])[CH:37]=2)=[N:26][S:25](=O)[N:24]=1>>[NH2:22][C:23]1[C:27]([NH:28][CH2:29][CH2:30][S:31][CH2:32][C:33]2[S:34][C:35]([CH2:39][N:40]([CH3:41])[CH3:42])=[C:36]([CH3:38])[CH:37]=2)=[N:26][S:25][N:24]=1

Participants

3

Reactant 2

HCID 23312524HCID 23312524, compoundHCID 23312529HCID 23312529, compound

Product 1

HCID 23312521HCID 23312521, compound

Procedure

The general procedure of Example 5 is repeated except that the 3-amino-4-{2-[(5-dimethylaminomethyl-3-thienyl)methylthio]ethylamino}-1,2,5-thiadiazole 1-oxide utilized therein is replaced by an equimolar amount of 3-amino-4-{2-[(5-dimethylaminomethyl-4-methyl-2-thienyl)methylthio]ethylamino}-1,2,5-thiadiazole 1-oxide [prepared according to the general procedure described in U.S. Pat. No. 4,374,248], and the title compound is thereby produced.

Workup

  1. customprepared

Sources & evidence

ORD record
ord-01957a376c9e45258e2f908a945361ab
Source dataset
uspto-grants-1984_04
Patent number
US04440933

Reaction notes

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