Sodium Hydroxide → HCID 23707418, compound

HRID 325549Notes

Reaction equation

HRID 325549 reaction equation
[CH2:1]([NH:4][C:5]1[CH:6]=[C:7]([CH2:11][C:12]([OH:14])=[O:13])[CH:8]=[CH:9][CH:10]=1)[CH:2]=[CH2:3].[OH-].[Na+:16]>O.C(O)C>[CH2:1]([NH:4][C:5]1[CH:6]=[C:7]([CH2:11][C:12]([O-:14])=[O:13])[CH:8]=[CH:9][CH:10]=1)[CH:2]=[CH2:3].[Na+:16]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 13293047HCID 13293047, compound

Product 1

HCID 23707418HCID 23707418, compound

Reagents, catalysts & solvents 1

HCID 19096565Water ethanolSolvent

Procedure

A mixture of 3.62 g. of 3-(allylamino)phenylacetic acid and 25 ml. of ethanol water (9:1) containing 0.400 g. of sodium hydroxide is stirred for 4 hours. The mixture is filtered and the residue washed with 10 ml. of ethanol-water (9:1) and dried in vacuo for 24 hours to yield sodium 3-(allylamino)phenylacetate as a white solid.

Workup

  1. additionA mixture of 3.62 g
  2. filtrationThe mixture is filtered
  3. washthe residue washed with 10 ml
  4. dry with materialof ethanol-water (9:1) and dried in vacuo for 24 hours

Sources & evidence

ORD record
ord-aacaca8e9c894f65809ba910b5d2830f
Source dataset
uspto-grants-1984_04
Patent number
US04440940

Reaction notes

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