HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Dodecanol → p-Dioxanone 2,5-Morpholinedione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Dodecanol | HCID 8193 | — |
| Reactant | 2-ethylhexanoic acid tin(II) salt | HCID 9318 | — |
| Reactant | Morpholine-2,5-dione | HCID 1714329 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | p-Dioxanone 2,5-Morpholinedione | HCID 69494823 | — |
Reaction Steps
P-Dioxanone (255.4 g, 2.504 moles), 2.5-morpholinedione (12.0 g, 0.104 moles), 1-dodecanol (0.763 g, 0.00409 moles) and a catalytic amount of stannous octoate (0.525 ml of a 0.33 M toluene solution, 0.000173 moles) are heated and magnetically mixed in a flame and vacuum dried, sealed glass ampoule according to the following temperature/time scheme:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04441496 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-9ef56cbfff604edeaaea4adac71da837 |
| Source note | uspto-grants-1984_04 |