Benzylamine → N-benzyl-N-[thieno[2,3-d]pyrimidin-6-ylmethylidene]amine

HRID 32561Notes

Reaction equation

HRID 32561 reaction equation
CO[C:3]1[CH:4]=[C:5]([CH:18]=[CH:19][C:20]=1OC)[CH2:6][N:7]=[CH:8][C:9]1[S:17][C:12]2[N:13]=[CH:14][N:15]=[CH:16][C:11]=2[CH:10]=1.C(N)C1C=CC=CC=1>>[CH2:6]([N:7]=[CH:8][C:9]1[S:17][C:12]2[N:13]=[CH:14][N:15]=[CH:16][C:11]=2[CH:10]=1)[C:5]1[CH:4]=[CH:3][CH:20]=[CH:19][CH:18]=1

Participants

3

Reactant 2

HCID 7504BenzylamineHCID 17965764N-(3,4-dimethoxybenzyl)-N-[thieno[2,3-d]pyrimidin-6-ylmethylidene]amine

Product 1

HCID 69194866N-benzyl-N-[thieno[2,3-d]pyrimidin-6-ylmethylidene]amine

Procedure

The title compound was prepared by a similar process to that described for Intermediate 14 but using benzylamine in place of 3,4-dimethoxybenzylamine. Pale yellow solid (69 mg, 100%), which was used directly without further purification.

Workup

  1. customPale yellow solid (69 mg, 100%), which was used directly without further purification

Sources & evidence

ORD record
ord-380526473e64476f96944287284f4188
Source dataset
uspto-grants-2008_09
Patent number
US07427616B2

Reaction notes

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