HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 12741431, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Dipropylamine | HCID 8902 | — |
| Reactant | HCID 70501721 | HCID 70501721 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 12741431 | HCID 12741431 | — |
Reaction Steps
A mixture of 20 g of 7-methoxytetrahydronaphthalen-2-one and 20 ml of dipropylamine in 200 ml of benzene is heated under reflux for 15 hours with 500 mg of para-toluenesulphonic acid, the water of condensation being distilled off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04442126 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-8309b20552054ce4bc9a20f5832ac51b |
| Source note | uspto-grants-1984_04 |