HCID 20463977, compound → HCID 20463966, compound

HRID 325674Notes

Reaction equation

HRID 325674 reaction equation
[C:1]([NH:5][CH:6]1[CH2:15][CH2:14][C:13]2[C:8](=[CH:9][CH:10]=[C:11]([O:19][CH3:20])[C:12]=2[N+:16]([O-])=O)[CH2:7]1)(=[O:4])[CH2:2][CH3:3]>CO>[C:1]([NH:5][CH:6]1[CH2:15][CH2:14][C:13]2[C:8](=[CH:9][CH:10]=[C:11]([O:19][CH3:20])[C:12]=2[NH2:16])[CH2:7]1)(=[O:4])[CH2:2][CH3:3]

Participants

3

Reactant 1

HCID 20463977HCID 20463977, compound

Product 1

HCID 20463966HCID 20463966, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1.8 g of the isomer nitrated in the 5-position, prepared as described in (b) above, in suspension in 50 ml of methanol, are hydrogenated under the conditions of Example 1(d). After the catalyst has been filtered off and the solvent has been evaporated off, 1.4 g of a product, melting at 141° C., are collected.

Workup

  1. customprepared
  2. filtrationAfter the catalyst has been filtered off
  3. customthe solvent has been evaporated off
  4. custom1.4 g of a product, melting at 141° C., are collected

Sources & evidence

ORD record
ord-1d8f5572c6b547c798155101df9faab9
Source dataset
uspto-grants-1984_04
Patent number
US04442126

Reaction notes

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