HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl N-cyanodithioiminocarbonate → methyl N-cyano-1-methyl-2-(phenylmethylene)-hydrazinecarboximidothioate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl N-cyanodithioiminocarbonate | HCID 66289 | — |
| Reactant | Benzaldehyde Methylhydrazone | HCID 302615 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | methyl N-cyano-1-methyl-2-(phenylmethylene)-hydrazinecarboximidothioate | HCID 54323404 | — |
Reaction Steps
A mixture of cyanocarbonimidodithioic acid dimethyl ester (1.46 g) and benzaldehyde N-methyl hydrazone (1.34 g) in acetonitrile was heated under reflux for 50 hr. The reaction mixture was cooled to 25° to give the title compound as colourless crystals, m.p. 132°-133° (0.73 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04442110 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-8cc709ba384141cead96102ce0cdebb6 |
| Source note | uspto-grants-1984_04 |