HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-((3-bromophenyl)(tosyl)methyl)formamide → 1-Bromo-3-(isocyano(tosyl)methyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-((3-bromophenyl)(tosyl)methyl)formamide | HCID 11337611 | — |
| Reactant | (3-Iodophenyl)(isocyano)methyl 4-methylphenyl sulfone | HCID 17965763 | — |
| Reactant | {(3-Iodophenyl)[(4-methylphenyl)sulfonyl]methyl}formamide | HCID 85929703 | — |
| Product | 1-Bromo-3-(isocyano(tosyl)methyl)benzene | HCID 2771785 | — |
Reaction Steps
The title compound was prepared by a similar process to that described for Intermediate 53 but using {(3-bromophenyl)[(4-methylphenyl)sulfonyl]methyl}formamide (Intermediate 56) in place of {(3-iodophenyl)[(4-methylphenyl)sulfonyl]methyl}formamide (Intermediate 52). Light brown solid (3.2 g, 30%);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07427616B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-14662cabbe2e4582ba1fa9fd3dbb6c38 |
| Source note | uspto-grants-2008_09 |