HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → N-cyano-1-methylhydrazinecarboximidothioic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | Dimethyl N-cyanodithioiminocarbonate | HCID 66289 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-cyano-1-methylhydrazinecarboximidothioic acid methyl ester | HCID 86738283 | — |
Reaction Steps
A mixture of methyl hydrazine (0.48 ml) and cyanocarbonimidodithioic acid dimethyl ester (1.3 g) in acetonitrile was stirred at 25° for 16 hours. The resulting solution was evaporated to a gum which was crystallized from acetonitrile/ether to give the title compound as colourless granules (210 mg) m.p. 69°-71°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04442110 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-c78b6c0c00204b74937009c72eff7aa6 |
| Source note | uspto-grants-1984_04 |