HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Iodophenyl)(isocyano)methyl 4-methylphenyl sulfone → (4-Iodophenyl)(isocyano)methyl 4-methylphenyl sulfone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Iodophenyl)(isocyano)methyl 4-methylphenyl sulfone | HCID 17965763 | — |
| Reactant | {(3-Iodophenyl)[(4-methylphenyl)sulfonyl]methyl}formamide | HCID 85929703 | — |
| Reactant | {(4-Iodophenyl)[(4-methylphenyl)sulfonyl]methyl}formamide | HCID 85929719 | — |
| Product | (4-Iodophenyl)(isocyano)methyl 4-methylphenyl sulfone | HCID 17965860 | — |
Reaction Steps
The title compound was prepared by a similar process to that described for Intermediate 53 but using {(4-iodophenyl)[(4-methylphenyl)sulfonyl]methyl}formamide (Intermediate 60) in place of {(3-iodophenyl)[(4-methylphenyl)sulfonyl]methyl}formamide (Intermediate 52). Brown gum (3.1 g, 20%);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07427616B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-ed733fabd8514a70b098bfd93c339921 |
| Source note | uspto-grants-2008_09 |