HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → 4-(1-Pyrrolyl)-1-indanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-(1-Pyrrolyl)-1-indanyl acetate | HCID 13239580 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-(1-Pyrrolyl)-1-indanol | HCID 13102461 | 27% |
Reaction Steps
In the manner of Example 1, step H, hydrolysis of 13.0 g (0.054 mole) of 4-(1-pyrrolyl)-1-indanyl acetate with 4.3 g of potassium hydroxide in 77 mL of water and 154 mL of ethanol gave 2.9 g of 4-(1-pyrrolyl)-1-indanol, m.p. 80°-81° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04442296 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-83305048e44643a6a31de8fbe3d5345f |
| Source note | uspto-grants-1984_04 |