HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → N-(2-Aminoethyl)-2-(2,6-dichlorophenoxy)propanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | Ethyl 2-(2,6-dichlorophenoxy)propanoate | HCID 13177850 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-(2-Aminoethyl)-2-(2,6-dichlorophenoxy)propanamide | HCID 13177851 | 76.7% |
Reaction Steps
42.0 g (=0.160 mols) of (+)-2-(2,6-dichlorophenoxy)-propionic acid ethylester are stirred for 6 hours at room temperature with 194.0 g (=3.228 mols) of 1,2-diaminoethane and, after working up, produce 34.0 g of (+)-2-(2,6-dichlorophenoxy)-propionic acid-N-(2-aminoethyl)amide, C11H14Cl2N2O2 [277.2] as a high viscosity oil, [α]D20 =+5.6° (c=1/ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04443464 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-3a08fc7097a44d909070b63b9c8caf22 |
| Source note | uspto-grants-1984_04 |