Formamide → HCID 178478096, compound

HRID 325951Notes

Reaction equation

HRID 325951 reaction equation
[Cl:1][C:2]1[CH:13]=[CH:12][CH:11]=[C:10]([Cl:14])[C:3]=1[CH2:4][C:5]1[N:6]=[CH:7]O[CH:9]=1.C([NH2:17])=O>O>[Cl:1][C:2]1[CH:13]=[CH:12][CH:11]=[C:10]([Cl:14])[C:3]=1[CH2:4][C:5]1[N:6]=[CH:7][NH:17][CH:9]=1

Participants

4

Reactant 2

HCID 713FormamideHCID 204633054-(2',6'-Dichlorobenzyl)oxazole

Product 1

HCID 178478096HCID 178478096, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
180 °C

Procedure

A mixture of 10 g of 4-(2',6'-dichlorobenzyl)oxazole and 30 ml of formamide is stirred at 180° C. for 4 hours. The mixture is cooled and diluted with water. The reaction product is thereafter isolated in the same manner as described in Example 49(d).

Workup

  1. temperatureThe mixture is cooled
  2. customThe reaction product is thereafter isolated in the same manner

Sources & evidence

ORD record
ord-ecce5756c6044e02b7ffaa810eb17ea9
Source dataset
uspto-grants-1984_04
Patent number
US04443466

Reaction notes

Loading…