HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzyl-4-[(2-methylphenyl)methyl]-1H-imidazole → HCID 178424218, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzyl-4-[(2-methylphenyl)methyl]-1H-imidazole | HCID 70503216 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178424218 | HCID 178424218 | — |
Reaction Steps
12.3 g of N-benzyl-4-(2'-methylbenzyl)imidazole are dissolved in 100 ml of ethanol. 0.3 g of 10% palladium-on-carbon is added and the reaction mixture is stirred vigorously at 70° C. in a hydrogen atmosphere until the uptake of hydrogen ceases. The mixture is cooled and filtered. Subsequent treatment as described in Example 54 above affords the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04443466 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-50e43f20e5514462bcd7901700657952 |
| Source note | uspto-grants-1984_04 |