HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethylbutyraldehyde → 3,7-Diethyl-5-azanona-3,5-diene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethylbutyraldehyde | HCID 7359 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Product | 3,7-Diethyl-5-azanona-3,5-diene | HCID 12413470 | 76.5% |
Reaction Steps
To a sample of 250 grams of 28% ammonium hydroxide was added 215 grams of 2-ethylbutyraldehyde and the heterogeneous mixture was stirred for 18 hours at ambient temperature. The resulting organic layer was separated, and after drying, slowly distilled at atmospheric pressure to yield 148.8 grams of 3,7-diethyl-5-azanona-3,5-diene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04443609 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-7485e4e1d9c24c839b4ca499287abe82 |
| Source note | uspto-grants-1984_04 |