HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 13472700, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 13472699 | HCID 13472699 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 13472700 | HCID 13472700 | 97.8% |
Reaction Steps
A mixture of 3-(4-methoxyphenoxy)quinoline (2.6 g), acetic acid (20 ml) and hydrobromic acid (20 ml of 48%) was boiled under reflux for 5 hours. The solution was concentrated under reduced pressure, poured onto ice and the resultant precipitate was collected by filtration to give 3-(4-hydroxyphenoxy)quinoline as a dark brown solid (2.4 g), mp 250° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04444584 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-218c51b6944e45a599014178ea4aa1f6 |
| Source note | uspto-grants-1984_04 |